Indexed by:
期刊论文
First Author:
Zhang, Xiaodong
Correspondence Author:
Qu, ZP (reprint author), Dalian Univ Technol, Key Lab Ind Ecol & Environm Engn MOE, Sch Environm Sci & Technol, Linggong Rd 2, Dalian 116024, Peoples R China.
Co-author:
Qu, Zhenping,Li, Xinyong,Zhao, Qidong,Zhang, Xin,Quan, Xie
Date of Publication:
2011-06-30
Journal:
MATERIALS LETTERS
Included Journals:
SCIE、EI
Document Type:
J
Volume:
65
Issue:
12
Page Number:
1892-1895
ISSN No.:
0167-577X
Key Words:
Nanocomposites; In-situ synthesis; pH-adjusting; Porous materials;
Ag/SBA-15
Abstract:
Ag nanoparticles were incorporated into the channels of mesoporous SBA-15 by the "pH-adjusting" method. In this procedure, the pH value of the solution was adjusted up to 7.5 by adding ammonia. The structural properties of Ag/SBA-15 nanocomposites were systematically investigated by X-ray powder diffraction (XRD), Transmission electron microscope (TEM). N(2) adsorption-desorption isotherms. inductively coupled plasma atomic emission spectroscopy (ICP-AES) and Fourier transform infrared spectroscopy (FT-IR) techniques. The characterization results reveal that the synthesized materials exhibit highly ordered hexagonal mesoporous structures, and highly dispersed Ag nanoparticles are confined inside the mesopores. It is the first time to report such high Ag loading on oxides fabricated by in-situ pH-adjusting method. (C) 2011 Elsevier B.V. All rights reserved.
Translation or Not:
no
