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Process parameters optimization of the MTBE reactive distillation by orthogonal numberical test and least square method
Release time:2019-11-07 Hits:
Indexed by: 期刊论文
First Author: Xiao, W.
Correspondence Author: Xiao, W (reprint author), Dalian Univ Technol, State Key Lab Fine Chem, R&D Ctr Membrane Sci & Technol, Dalian 116024, Liaoning, Peoples R China.
Co-author: Zhou, Y.,Du, S.,He, G.
Date of Publication: 2012-07-13
Journal: Advanced Materials Research
Included Journals: EI、CPCI-S
Document Type: J
Volume: 550-553
Page Number: 947-952
ISSN No.: 9783037854556
Key Words: Reactive distillation; Parameter optimization; Orthogonal numerical test; Least square method; MTBE
Abstract: Because of the large number of operating and equipment parameters of the reactive distillation(RD) and a strong coupling between them, it is difficult to find the optimal process parameters. A novel hybrid method on process parameters optimization of methyl tertiary butyl ether (MTBE) RD was developed in the paper. MTBE RD process was firstly simulated with Aspen Plus. Then based on the MTBE RD model, sensitivity analysis of various parameters was accomplished to determine the key decision parameters. After that, the orthogonal numerical tests were performed in feasible fields to obtain nearly optimal parameters. Finally, with the orthogonal numerical test results, the least square method was used to regress equation, which showed the relationship between objective function and the key decision parameters, thus determining the optimal operating parameters and equipment parameters. Results of analysis indicated that the combination of orthogonal numerical test and the least square method can be attractive since the number of tests was reduced substantially while the specification of the products can be met.
Translation or Not: no